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dc.contributor.authorBisgin, Abdullah Taner
dc.contributor.authorSurme, Yavuz
dc.contributor.authorUcan, Mustafa
dc.contributor.authorNarin, Ibrahim
dc.date.accessioned2019-08-01T13:38:39Z
dc.date.available2019-08-01T13:38:39Z
dc.date.issued2016
dc.identifier.issn0717-9707
dc.identifier.urihttps://hdl.handle.net/11480/3635
dc.descriptionWOS: 000389063200028en_US
dc.description.abstractAn effective extraction procedure based on the complexation of Cu2+, Cd2+, and Ni2+ with dithizone and extraction of these complexes by Tergitol NP-7 surfactant was developed. Micelle mediated extraction parameters such as pH, ligand and surfactant concentration, incubation time and temperature were investigated and optimized. Effects of external and internal interfering ions, linear dynamic range, detection and quantitation limits were examined and determined under optimal conditions. Detection limits were found as 0.5, 1.8 and 2.0 mg L-1 for Cu2+, Ni2+ and Cd2+, respectively. Linear dynamic range values were between 0.125-2, 0.125-2.5 and 0.05-1.4 mu g mL(-1) for Cu2+, Ni2+ and Cd2+ ions, respectively. Applicability, accuracy and precision of the method were checked with standard reference materials and real sample analyses by analyte addition technique. Finally, optimized method was applied to determine Cu2+, Ni2+ and Cd2+ contents of standard reference materials, mushrooms and water samples. Quantitative and accurate results were obtained from the analysis of standard reference materials and real samples.en_US
dc.description.sponsorshipNigde University Scientific Research Projects Unit (BAGEP Project) [FEB-2015/40]en_US
dc.description.sponsorshipThe authors are grateful to the Nigde University Scientific Research Projects Unit (BAGEP Project number: FEB-2015/40) for its financial support.en_US
dc.language.isoengen_US
dc.publisherSOC CHILENA QUIMICAen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectMicelle mediated extractionen_US
dc.subjectDithizoneen_US
dc.subjectFAASen_US
dc.subjectHeavy metalsen_US
dc.subjectTergitol NP-7en_US
dc.titleSIMULTANEOUS PRECONCENTRATION AND DETERMINATION OF Cu2+, Ni2+ AND Cd2+ BY MICELLE MEDIATED EXTRACTION IN FOOD AND WATER SAMPLESen_US
dc.typearticleen_US
dc.relation.journalJOURNAL OF THE CHILEAN CHEMICAL SOCIETYen_US
dc.departmentNiğde ÖHÜen_US
dc.identifier.volume61en_US
dc.identifier.issue2en_US
dc.identifier.startpage2990en_US
dc.identifier.endpage2995en_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.contributor.institutionauthor[0-Belirlenecek]


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